![]() Method of separating hydrocarbon mixture
专利摘要:
The invention relates to refrigeration. The purpose of the invention is to reduce energy consumption and simplify the technological scheme. The mixture containing carbon dioxide is cooled and partially condensed in cooler 2, from which, as a mixture, gas-liquid enters separator 3 where it is separated. From the separator, gas and liquid are separated in separate streams into distillation column 6. Using heater 7, some of the liquid in the lower part of the column is evaporated, gas rises through the column, enriched with light hydrocarbons and removed as a product. Condensate for irrigation columns are cooled to m-ry -30 ... +30 C and served from its bottom. From the middle part of the column below the level of the gas and liquid inlet, the gaseous side fraction is withdrawn and condensed under pressure. 3 з, п, ф-л, 1 Il. to CO 公开号:SU1438628A3 申请号:SU864027950 申请日:1986-08-04 公开日:1988-11-15 发明作者:Ранке Герхард;Диль Эльмар 申请人:Линде Аг (Фирма); IPC主号:
专利说明:
J-: i Chii about 6 W Yu zL 1. I I fS /four GU L te 1438628 j The invention relates to a refrigeration engineering, in particular to a technique for separating mixtures of hydrocarbons by the method of cooling and rectification, The purpose of the invention is to reduce energy consumption and simplify the technological scheme. The drawing shows an installation diagram which allows to realize the proposed method of separation of the mixture, The installation contains a mixture supply pipeline 1, a cooler 2, a separator 3 connected by pipelines 4 and 5, delivering gas and liquid to the rectification column 6, a heater 7 is installed in the lower part of the column 6,: Pipe 6 and 8 are installed on the column 6 pipeline Part of the liquid from fraction C. from the lower part of the column through line 11 through cooler 12 is fed to the irrigation of column 6 and flows down the plates, washing the fraction into the lower part of the column. From the middle part of the column below the liquid and gas injection level, the product Cj + as side fraction is withdrawn through line 9. Part C of the C fraction from the bottom part of the column is withdrawn as product by line 16.
权利要求:
Claims (4) [1] 1. A method for separating a mixture of hydrocarbons, in particular containing coal acid gas, by cooling it with | 10 condensate removal from the bottom, 20 partial condensation and production through pipe 11, condensate from the bottom of the column is fed to the column for irrigation through cooler 12. The dashed lines show the gas distributor plate 13, the pipeline 14 25 | and the heat exchanger 15. Through the pipeline 16, the condensate in the form of the product withdraws from the column 6. The installation works as follows | 3th. thirty ; Pipeline 1 contains a gas mixture | hydrocarbons with a high content of fraction C. The chiller 2 comes to cooling, where it is partially condensed by the side-: its cold source and the gas-liquid mixture flows into the separator 3, in which divided into liquid and gas. I From the separator 3, gas and liquid are supplied via Piping 4 and 5 to the distillation column according to their composition and temperatures. With the help of a heater, 7 of the liquid in the lower part of the column is vaporized, the gas 35 40 gas-liquid mixtures; separating a mixture of gas and liquid inlet into separate distillation column into a distillation column; condensation column reflux; gas from the upper part of the column containing light hydrocarbons and in particular carbon dioxide; and from the lower part of the column — condensate containing heavy hydrocarbons, which are used in order to reduce energy consumption and simplify the technological scheme, condensate is supplied from the bottom of the column for irrigation of the column. [2] 2. Method POP.1, characterized in that a gaseous side fraction is withdrawn from the middle part of the column below the gas and liquid inlets [3] 3. Method according to claim 2, characterized in that the side fraction is condensed under pressure. [4] 4. Method pop.1, I distinguish It enters the column 6, enriches - 45 u and the condensate, the liquid of the fraction C from the bottom of the column through line 11 through the cooler 12 is fed to the irrigation of the column 6 and flows down the plates, washing the fraction into the lower part of the column. From the middle part of the column below the level of liquid and gas input, the product Cj + as side fraction is withdrawn via line 9. Part C of the C fraction from the bottom part of the column is diverted as product 16 via line 16. Invention Formula 1. A method for separating a mixture of hydrocarbons, in particular carbon dioxide-containing gas, by cooling it with partial condensation and production gas – liquid mixtures; separating the mixture, introducing gas and liquid in separate streams into the distillation column for separation, refluxing the column with condensate, for withdrawing from the upper part of the column a gas containing light hydrocarbons and in particular carbon dioxide, and from the lower part of the column for condensate containing heavy hydrocarbons, which are used in order to reduce energy consumption and simplify the technological scheme, condensate is supplied from the bottom of the column for irrigation of the column. 2. Method POP1, characterized in that a gaseous side fraction is withdrawn from the middle part of the column below the gas and liquid inlets. 3. Method according to claim 2, characterized in that the side fraction is condensed under pressure. 4. Method pop.1, I distinguish
类似技术:
公开号 | 公开日 | 专利标题 SU1438628A3|1988-11-15|Method of separating hydrocarbon mixture SU1704646A3|1992-01-07|Method for separating gaseous mixture which contains carbon dioxide and light hydrocarbons US6442969B1|2002-09-03|Process and device for separation of at least one acid gas that is contained in a gas mixture US2777305A|1957-01-15|Separation and recovery of ethylene US7129387B2|2006-10-31|Low capital implementation of distributed distillation in ethylene recovery US2815650A|1957-12-10|Reboiled absorber operation US2475957A|1949-07-12|Treatment of natural gas US3417572A|1968-12-24|Separation of hydrogen sulfide from carbon dioxide by distillation US2690060A|1954-09-28|Fractional distillation RU2688533C1|2019-05-21|Ltdr plant for integrated gas preparation and production of lng and its operation method US2551399A|1951-05-01|Process for the purification of carbon dioxide US2214790A|1940-09-17|Process and apparatus for separating gases EP0134243B1|1988-07-27|Apparatus and method for recovering light hydrocarbons from hydrogen containing gases US3512368A|1970-05-19|Helium and nitrogen containing fuel product recovery US3214890A|1965-11-02|Method of separation of hydrocarbons by a single absorption oil US3444072A|1969-05-13|Method for minimizing hydrogen losses in high pressure processes US5389242A|1995-02-14|Process for the fractionation of oil and gas on a petroleum deposit effluent US3238735A|1966-03-08|Distillation of low-boiling components US1843043A|1932-01-26|Process for the separation of the several components of gaseous mixtures US2502251A|1950-03-28|Apparatus for the separation of gaseous mixtures US1784120A|1930-12-09|Separation of the constituents of gaseous mixtures US3390534A|1968-07-02|Method for separation of multicomponent mixtures US2168683A|1939-08-08|Absorption process US2230619A|1941-02-04|Process for separating gas and oil SU1645796A1|1991-04-30|Process of simultaneous production of heliun ethan and heavier hydrocarbons
同族专利:
公开号 | 公开日 GB2178445A|1987-02-11| GB8619083D0|1986-09-17| NO863146D0|1986-08-04| US4881960A|1989-11-21| NO863146L|1987-02-06| NL8601999A|1987-03-02| DE3528071A1|1987-02-05| IN168463B|1991-04-06| GB2178445B|1989-08-16|
引用文献:
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申请号 | 申请日 | 专利标题 DE19853528071|DE3528071A1|1985-08-05|1985-08-05|METHOD FOR DISASSEMBLING A HYDROCARBON MIXTURE| 相关专利
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